N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Base Information

Chemical Name:N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester
CAS No.:430474-80-9
Molecular Formula:C₂₃H₂₈N₂O₇
Molecular Weight:444.485
Hs Code.:

Synonyms:N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Suppliers and Price of N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

There total 4 articles about N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 430474-79-6
N-(benzyl 2-carbobenzyloxyamino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

: 430474-80-9
N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 1h;
DOI:10.7164/antibiotics.55.191

Reference yield:

: 4713-66-0
benzyl 2-carbobenzyloxyamino-2-deoxy-α-D-galactopyranoside

: 430474-80-9
N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / O₂; NaHCO₃ / Pt / H₂O / 5 h / 80 °C

2: 79 percent / 1-hydroxybenzotriazole; 1,3-dicyclohexylcarbodiimide / dimethylformamide / 18 h / 20 °C

3: 96 percent / H₂ / 10 percent Pd/C / methanol / 1 h / 20 °C

With hydrogen; oxygen; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; platinum; In methanol; water; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.55.191

Reference yield:

: 3006-58-4
2-carbobenzyloxyamino-2-deoxy-D-galactopyranose

: 430474-80-9
N-(benzyl 2-amino-2-deoxy-α-D-galactopyranosiduronyl)-β-D-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / acetyl chloride / 1.5 h / 80 °C

2: 97 percent / O₂; NaHCO₃ / Pt / H₂O / 5 h / 80 °C

3: 79 percent / 1-hydroxybenzotriazole; 1,3-dicyclohexylcarbodiimide / dimethylformamide / 18 h / 20 °C

4: 96 percent / H₂ / 10 percent Pd/C / methanol / 1 h / 20 °C

With hydrogen; oxygen; sodium hydrogencarbonate; benzotriazol-1-ol; acetyl chloride; dicyclohexyl-carbodiimide; palladium on activated charcoal; platinum; In methanol; water; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.55.191