C₂₉H₂₇N₃O₄S₂

Base Information

Chemical Name:C₂₉H₂₇N₃O₄S₂
CAS No.:1333378-21-4
Molecular Formula:C₂₉H₂₇N₃O₄S₂
Molecular Weight:545.683
Hs Code.:

C<sub>29</sub>H<sub>27</sub>N<sub>3</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₉H₂₇N₃O₄S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₇N₃O₄S₂

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Technology Process of C₂₉H₂₇N₃O₄S₂

There total 11 articles about C₂₉H₂₇N₃O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1094172-58-3
C₁₁H₁₃BN₂O₃S

: 1333378-20-3
C₁₈H₁₆BrNO₃S

: 1333378-21-4
C₂₉H₂₇N₃O₄S₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; water; at 100 ℃; for 24h;
DOI:10.1002/ejoc.201100242

Reference yield:

: C₁₃H₁₅BrN₂O₃

: 1333378-21-4
C₂₉H₂₇N₃O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

5.1: hydrogen bromide; acetic acid / tetrahydrofuran / 0.25 h / 0 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane; water / 24 h / 100 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; hydrogen bromide; sodium hydride; caesium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; water; mineral oil; 3.1: Sonogashira coupling / 6.1: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242

Reference yield:

: C₁₃H₁₇BN₂O₃S

: 1333378-21-4
C₂₉H₂₇N₃O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran; hexane

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane; water / 24 h / 100 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; caesium carbonate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; hexane; water; 2: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242