5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

Base Information

Chemical Name:5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester
CAS No.:93018-74-7
Molecular Formula:C₁₆H₁₈INO₆
Molecular Weight:447.227
Hs Code.:

5<i>t</i>-acetoxy-2-benzoyl-4<i>c</i>-iodo-3<i>c</i>-methyl-[1,2]oxazinane-6<i>r</i>-carboxylic acid methyl ester

Synonyms:5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

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Chemical Property of 5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

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Technology Process of 5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

There total 5 articles about 5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 689-89-4
(2E,4E)-methylhexa-2,4-dienoate

: 93018-74-7
5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether; ethanol / 336 h / 0 °C

2: aq. NaHCO₃

3: (i) Na₂HPO₄, ClCH₂CH₂Cl, (ii) H₂O₂, ClCH₂CH₂Cl, (CF₃CO)2O

4: aq. HI

5: Py, DMF

With pyridine; hydrogen iodide; sodium hydrogencarbonate; N,N-dimethyl-formamide; In diethyl ether; ethanol;
DOI:10.1021/ja00884a013

Reference yield:

: 412338-32-0
3,6-dihydro-6-methoxycarbonyl-3-methyl-2H-1,2-oxazine

: 93018-74-7
5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaHCO₃

2: (i) Na₂HPO₄, ClCH₂CH₂Cl, (ii) H₂O₂, ClCH₂CH₂Cl, (CF₃CO)2O

3: aq. HI

4: Py, DMF

With pyridine; hydrogen iodide; sodium hydrogencarbonate; N,N-dimethyl-formamide;
DOI:10.1021/ja00884a013

Reference yield:

: 92249-11-1
2-benzoyl-3c-methyl-3,6-dihydro-2H-[1,2]oxazine-6r-carboxylic acid methyl ester

: 93018-74-7
5t-acetoxy-2-benzoyl-4c-iodo-3c-methyl-[1,2]oxazinane-6r-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Na₂HPO₄, ClCH₂CH₂Cl, (ii) H₂O₂, ClCH₂CH₂Cl, (CF₃CO)2O

2: aq. HI

3: Py, DMF

With pyridine; hydrogen iodide; N,N-dimethyl-formamide;
DOI:10.1021/ja00884a013