Technology Process of C6(C6H4CH3)3(C6H4C3H4NO)3
There total 3 articles about C6(C6H4CH3)3(C6H4C3H4NO)3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
dicobalt octacarbonyl;
In
1,4-dioxane;
at 110 ℃;
for 64h;
DOI:10.1021/ja064194f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 86 percent / NaOMe / 1 h / 70 °C
2: DMAP; Et3N / CH2Cl2 / 20 h / 20 °C
3: 85 percent / NaOH / methanol / 2 h / 20 °C
4: 75 percent / CuI; Et3N / PdCl2(PPh3)2 / 12 h / 70 °C
5: 6 percent / Co2(CO)8 / dioxane / 64 h / 110 °C
With
dmap; sodium hydroxide; copper(l) iodide; sodium methylate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; dicobalt octacarbonyl;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ja064194f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: DMAP; Et3N / CH2Cl2 / 20 h / 20 °C
2: 85 percent / NaOH / methanol / 2 h / 20 °C
3: 75 percent / CuI; Et3N / PdCl2(PPh3)2 / 12 h / 70 °C
4: 6 percent / Co2(CO)8 / dioxane / 64 h / 110 °C
With
dmap; sodium hydroxide; copper(l) iodide; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; dicobalt octacarbonyl;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/ja064194f