dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

Base Information

Chemical Name:dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate
CAS No.:709026-89-1
Molecular Formula:C₂₈H₅₀NO₇P
Molecular Weight:543.681
Hs Code.:

Synonyms:dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

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Chemical Property of dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

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Technology Process of dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

There total 5 articles about dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102308-32-7
(4S)-4-formyl-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 709026-89-1
dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: n-BuLi / tetrahydrofuran / -42 °C

2: PCC / CH₂Cl₂ / 20 °C

3: DIBAL-H / tetrahydrofuran / 0 °C

4: aq. AcOH; LiCl / 20 °C

5: CBr₄; pyridine / 0 °C

With pyridine; n-butyllithium; carbon tetrabromide; diisobutylaluminium hydride; acetic acid; pyridinium chlorochromate; lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2004.03.001

Reference yield:

: 309919-02-6
1-bromo-3-dodecylbenzene

: 709026-89-1
dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: n-BuLi / tetrahydrofuran / -42 °C

2: PCC / CH₂Cl₂ / 20 °C

3: DIBAL-H / tetrahydrofuran / 0 °C

4: aq. AcOH; LiCl / 20 °C

5: CBr₄; pyridine / 0 °C

With pyridine; n-butyllithium; carbon tetrabromide; diisobutylaluminium hydride; acetic acid; pyridinium chlorochromate; lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2004.03.001

Reference yield:

: 309919-05-9
N-tert-butoxycarbonyl (4S)-4-(3'-dodecylbenzoyl)-2,2-dimethyl-1,3-oxazolidine

: 709026-89-1
dimethyl (2S,3R)-2-(tert-butoxycarbonylamino)-3-(hydroxy-3-dodecylphenyl)prop-1-ylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / tetrahydrofuran / 0 °C

2: aq. AcOH; LiCl / 20 °C

3: CBr₄; pyridine / 0 °C

With pyridine; carbon tetrabromide; diisobutylaluminium hydride; acetic acid; lithium chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2004.03.001