Technology Process of C19H24O5
There total 5 articles about C19H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; toluene;
at -78 - 20 ℃;
DOI:10.1021/jm301488q
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium methylate / dimethyl sulfoxide
2: camphor-10-sulfonic acid / dichloromethane / 20 °C
3: diisobutylaluminium hydride / tetrahydrofuran; methanol; toluene / -78 - 20 °C
With
camphor-10-sulfonic acid; sodium methylate; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jm301488q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C
1.2: 0.17 h
2.1: sodium methylate / dimethyl sulfoxide
3.1: camphor-10-sulfonic acid / dichloromethane / 20 °C
4.1: diisobutylaluminium hydride / tetrahydrofuran; methanol; toluene / -78 - 20 °C
With
oxalyl dichloride; camphor-10-sulfonic acid; sodium methylate; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm301488q