4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

Base Information

Chemical Name:4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one
CAS No.:214916-07-1
Molecular Formula:C₁₃H₁₂N₂O₃S₂
Molecular Weight:308.382
Hs Code.:

4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ<sup>6</sup>-dithia-5,7-diaza-inden-6-one

Synonyms:4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

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Chemical Property of 4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

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Technology Process of 4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

There total 4 articles about 4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 214916-03-7
4-Phenethylsulfamoyl-thiophene-3-carbonyl azide

: 214916-07-1
4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

Guidance literature:: In toluene; for 5h; Heating;
DOI:10.1021/jm9802012

Reference yield:

: 64-04-0
phenethylamine

: 214916-07-1
4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / K₂CO₃ / tetrahydrofuran / 1.) 5 deg C, 1 h, 2.) reflux, 6 h

2: 64 percent / H₂NNH₂*H₂O / ethanol / 1 h / Heating

3: 83 percent / aq. HCl, AcOH, NaNO₂ / 2 h / 10 °C

4: 70 percent / toluene / 5 h / Heating

With hydrogenchloride; potassium carbonate; hydrazine hydrate; acetic acid; sodium nitrite; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm9802012

Reference yield:

: 214915-91-0
4-Phenethylsulfamoyl-thiophene-3-carboxylic acid methyl ester

: 214916-07-1
4,4-Dioxo-5-phenethyl-4,5-dihydro-7H-2,4λ⁶-dithia-5,7-diaza-inden-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / H₂NNH₂*H₂O / ethanol / 1 h / Heating

2: 83 percent / aq. HCl, AcOH, NaNO₂ / 2 h / 10 °C

3: 70 percent / toluene / 5 h / Heating

With hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol; toluene;
DOI:10.1021/jm9802012