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Technology Process of {IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I

{IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I

Base Information
  • Chemical Name:{IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I
  • CAS No.:135107-61-8
  • Molecular Formula:C39H48IIrKN2O5P2*I
  • Molecular Weight:1171.9
  • Hs Code.:
{IrI(CO)K(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>(N((CH<sub>2</sub>)2O)2(CH<sub>2</sub>)2N(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)((CH<sub>2</sub>)2O)2(CH<sub>2</sub>)2))}<sup>(1+)</sup>*I<sup>(1-)</sup>={C<sub>39</sub>H<sub>48</sub>IIrKN<sub>2</sub>O<sub>5</sub>P<sub>2</sub>}I

Synonyms:{IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I

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Chemical Property of {IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I
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Technology Process of {IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I

There total 1 articles about {IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

{IrCl(CO)(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>(N(CH<sub>2</sub>)2O(CH<sub>2</sub>)2O(CH<sub>2</sub>)2N(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)(CH<sub>2</sub>)2O(CH<sub>2</sub>)2O(CH<sub>2</sub>)2))}
132673-23-5

{IrCl(CO)(P(C6H5)2CH2(N(CH2)2O(CH2)2O(CH2)2N(CH2P(C6H5)2)(CH2)2O(CH2)2O(CH2)2))}

{IrI(CO)K(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>(N((CH<sub>2</sub>)2O)2(CH<sub>2</sub>)2N(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)((CH<sub>2</sub>)2O)2(CH<sub>2</sub>)2))}<sup>(1+)</sup>*I<sup>(1-)</sup>={C<sub>39</sub>H<sub>48</sub>IIrKN<sub>2</sub>O<sub>5</sub>P<sub>2</sub>}I
135107-61-8

{IrI(CO)K(P(C6H5)2CH2(N((CH2)2O)2(CH2)2N(CH2P(C6H5)2)((CH2)2O)2(CH2)2))}(1+)*I(1-)={C39H48IIrKN2O5P2}I

Guidance literature:
With KI; In methanol; dichloromethane; (N2 atmosphere); a 5-fold excess of KI dissolved in MeOH is added to a soln. of Ir-complex in CH2Cl2, soln. is stirred for 1 h; solvents are removed by rotary evapn., residue is dissolved in CH2Cl2, filtn., dropwise addn. of Et2O, pptn., ppt. is collected by filtn., washed with Et2O, dried in vac., elem. anal.;
upstream raw materials:

{IrCl(CO)(P(C6H5)2CH2(N(CH2)2O(CH2)2O(CH2)2N(CH2P(C6H5)2)(CH2)2O(CH2)2O(CH2)2))}

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