tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate

Base Information

Chemical Name:tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate
CAS No.:105018-11-9
Molecular Formula:CH₂Cl₂*C₄₅H₄₈Cl₄N₆O₃Th
Molecular Weight:1179.7
Hs Code.:

Synonyms:tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate

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Chemical Property of tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate

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Technology Process of tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate

There total 1 articles about tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 33087-96-6,105018-10-8
tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV)

: 105018-11-9
tris(N,N'-dimethyl-N,N'-diphenylurea)tetrachlorothorium(IV) dichloromethane solvate

Guidance literature:: With CH₂Cl₂; In dichloromethane; byproducts: (CH3)(C6H5)NC(O)(CH3)(C6H5); addn. of n-pentane to Th complex in CH2Cl2 till soln. became cloudy; clearing by dropwise addn. of CH2Cl2; storage overnight; washing with n-pentane; drying in vac. for 5 h; elem. anal.;
DOI:10.1016/S0020-1693(00)84420-5