bufotalin 3-hemisuberate

Base Information

Chemical Name:bufotalin 3-hemisuberate
CAS No.:30219-15-9
Molecular Formula:C₃₄H₄₈O₉
Molecular Weight:600.75
Hs Code.:

Synonyms:bufotalin 3-hemisuberate

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Chemical Property of bufotalin 3-hemisuberate

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Technology Process of bufotalin 3-hemisuberate

There total 1 articles about bufotalin 3-hemisuberate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 571-31-3
Epietiocholanolone

: 30219-15-9
bufotalin 3-hemisuberate

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.1: palladium diacetate / dichloromethane; acetonitrile / 25 h / 20 °C / Inert atmosphere

4.1: silica gel; N-ethyl-N,N-diisopropylamine / 4 h / 80 °C / Inert atmosphere

5.1: oxygen; phenylsilane; cobalt(II) aceylacetonate / 1,4-dioxane / 5 h / 20 °C / 760.05 Torr

6.1: triethylamine; hydrazine hydrate / ethanol / 13 h / 50 °C / Inert atmosphere

6.2: 0.67 h / 0 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride / dimethyl sulfoxide; tetrahydrofuran / 13 h / 60 °C / Inert atmosphere

8.1: 3-chloro-benzenecarboperoxoic acid; sodium carbonate / dichloromethane / 5 h / -78 - -20 °C / Inert atmosphere

9.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

10.1: methanol; sodium tetrahydroborate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

11.1: pyridine / 18 h / 20 °C / Inert atmosphere

12.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 124 h / 20 °C / Inert atmosphere

13.1: dmap / dichloromethane / 11 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; methanol; dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; oxygen; palladium diacetate; silica gel; sodium carbonate; pyridine hydrogenfluoride; cobalt(II) aceylacetonate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; copper(l) chloride; lithium chloride; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.orglett.0c03251