ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate

Base Information

• Chemical Name: ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate
• CAS No.: 1147121-45-6
• Molecular Formula: C₁₈H₂₃NO₅S
• Molecular Weight: 365.45

Synonyms:ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate

Chemical Property of ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate

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Technology Process of ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate

There total 1 articles about ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

ethyl 4-[N-[(3,3-dimethyloxiran-2-yl)methyl]-(4-methylphenyl)sulfonylamino]-2-butynoate (1147121-38-7) → ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate (1147121-45-6)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; at 25 ℃; for 1h; Inert atmosphere;

DOI:10.1055/s-0031-1290466

Reference yield: 82.0%

ethyl [2-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-3,4-dihydro-2H-1,4-oxazin-6-yl]acetate (1147121-45-6) → [2-hydroxy-6-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-morpholin-2-yl]acetic acid (1147121-47-8)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2009.01.065

upstream raw materials:

ethyl 4-[N-[(3,3-dimethyloxiran-2-yl)methyl]-(4-methylphenyl)sulfonylamino]-2-butynoate

Downstream raw materials:

[2-hydroxy-6-(1-methylethenyl)-4-[(4-methylphenyl)-sulfonyl]-morpholin-2-yl]acetic acid

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