(Z)-diisopropyl styrylphosphonate

Base Information

Chemical Name:(Z)-diisopropyl styrylphosphonate
CAS No.:76371-53-4
Molecular Formula:C₁₄H₂₁O₃P
Molecular Weight:268.293
Hs Code.:

Synonyms:(Z)-diisopropyl styrylphosphonate

Suppliers and Price of (Z)-diisopropyl styrylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-diisopropyl styrylphosphonate

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-diisopropyl styrylphosphonate

There total 3 articles about (Z)-diisopropyl styrylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1809-20-7
diisopropyl hydrogenphosphonate

: 588-73-8,1340-14-3
(Z)-β-bromostyrene

: 76371-53-4
(Z)-diisopropyl styrylphosphonate

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 90 ℃; for 12h;
DOI:10.1016/0040-4039(80)80245-0

Reference yield:

: 1809-20-7
diisopropyl hydrogenphosphonate

: 7436-90-0
2,2-dibromostyrene

: 78463-00-0
diisopropyl (E)-(2-phenylethenyl)phosphonate

: 76371-53-4
(Z)-diisopropyl styrylphosphonate

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 120 ℃; for 24h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c0cc01617a

Reference yield:

: 116-17-6
triisopropyl phosphite

: 103-64-0,1340-14-3
bromostyrene

: 78463-00-0
diisopropyl (E)-(2-phenylethenyl)phosphonate

: 76371-53-4
(Z)-diisopropyl styrylphosphonate

Guidance literature:: With copper(l) iodide; In various solvent(s); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/a709082j