C₅₆H₆₅NO₉

Base Information

Chemical Name:C₅₆H₆₅NO₉
CAS No.:1262848-25-8
Molecular Formula:C₅₆H₆₅NO₉
Molecular Weight:896.133
Hs Code.:

C<sub>56</sub>H<sub>65</sub>NO<sub>9</sub>

Synonyms:C₅₆H₆₅NO₉

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Chemical Property of C₅₆H₆₅NO₉

Chemical Property:

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Technology Process of C₅₆H₆₅NO₉

There total 18 articles about C₅₆H₆₅NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1262848-05-4
C₁₁H₁₇IO₃

: 1262848-06-5
C₄₅H₄₇NO₆

: 1262848-25-8
C₅₆H₆₅NO₉

Guidance literature:: C₄₅H₄₇NO₆; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

C₁₁H₁₇IO₃; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol102856j

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 1262848-25-8
C₅₆H₆₅NO₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: cerium(III) chloride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.1: pyridine / 0.5 h / 20 °C / Inert atmosphere

3.1: ozone / dichloromethane / -78 °C

3.2: 17 h / -78 - 20 °C / Inert atmosphere

4.1: chromium dichloride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.2: 1 h / 20 °C / Inert atmosphere

With pyridine; chromium dichloride; cerium(III) chloride; ozone; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; 5.2: Suzuki-Miyaura coupling;
DOI:10.1021/ol102856j

Reference yield:

: 160836-05-5
C₂₁H₂₆O₅

: 1262848-25-8
C₅₆H₆₅NO₉

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / -5 - 0 °C / Inert atmosphere

2.1: 2,6-di-tert-butyl-4-methyl-phenol / tert-butylbenzene / 27 h / 180 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dichloro-ethane / 3 h / 40 °C / Inert atmosphere

4.1: methanesulfonamide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane] / water; tert-butyl alcohol / 62 h / 0 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.83 h / 20 °C / Inert atmosphere

7.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

8.1: magnesium bromide ethyl etherate / dichloromethane / 40 h / -10 °C / Inert atmosphere

9.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C / Inert atmosphere

10.1: hydrogenchloride; water / methanol / 16 h / 20 °C

11.1: triethylamine / dichloromethane / 0.5 h / 0 °C

12.1: sodium hydroxide / ethanol; water / 1 h / 80 °C

13.1: sodium hydroxide / water; ethyl acetate / 1.33 h / 0 - 20 °C

14.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

14.2: 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; methanesulfonamide; 2,6-di-tert-butyl-4-methyl-phenol; water; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium bromide ethyl etherate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; tert-butylbenzene; ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Overman rearrangement / 4.1: Sharpless dihydroxylation / 7.1: Swern oxidation / 8.1: Hosomi-Sakurai allylation / 14.2: Suzuki-Miyaura coupling;
DOI:10.1021/ol102856j