C₃₄H₄₆O₁₁

Base Information

Chemical Name:C₃₄H₄₆O₁₁
CAS No.:350583-33-4
Molecular Formula:C₃₄H₄₆O₁₁
Molecular Weight:630.733
Hs Code.:

C<sub>34</sub>H<sub>46</sub>O<sub>11</sub>

Synonyms:C₃₄H₄₆O₁₁

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Chemical Property of C₃₄H₄₆O₁₁

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Technology Process of C₃₄H₄₆O₁₁

There total 10 articles about C₃₄H₄₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 350583-32-3
C₄₀H₆₀O₁₁Si

: 350583-33-4
C₃₄H₄₆O₁₁

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: C₃₉H₄₄O₇

: 350583-33-4
C₃₄H₄₆O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1: 76 percent / aq. NaOH / tetrahydrofuran / 48 h / Heating

2: 93 percent / pyridine / 96 h / 20 °C

3: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

4: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

5: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

6: 70 percent / pyridine / 4 °C

7: 79 percent / imidazole / dimethylformamide / 20 °C

8: 39 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C

9: 43 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 24 h / 60 °C

10: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium hydroxide; osmium(VIII) oxide; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: 350583-27-6
1,2-benzylidene-9,10-isopropylidene-5α-acetyltaxicin-I

: 350583-33-4
C₃₄H₄₆O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

2: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

3: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

4: 70 percent / pyridine / 4 °C

5: 79 percent / imidazole / dimethylformamide / 20 °C

6: 39 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C

7: 43 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 24 h / 60 °C

8: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

With 1H-imidazole; tert.-butylhydroperoxide; osmium(VIII) oxide; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; pyridine; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O