{1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron

Base Information

• Chemical Name: {1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron
• CAS No.: 114410-62-7
• Molecular Formula: C₂₄H₂₉BN₄
• Molecular Weight: 384.332
• Mol file: 114410-62-7.mol

Synonyms:{1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron

Chemical Property of {1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron

There total 1 articles about {1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-diisopropylborylaminopyridine (114502-05-5) + 1,3-Diphenylcarbodiimide (622-16-2) → {1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron (114410-62-7)

Guidance literature:

In hexane; dropwise addn. of diimide in hexane to subst. pyridine in hexane at 25°C, pptn.; filtration, washing with hexane, elem. anal.;

DOI:10.1007/BF00956368

Reference yield: 96.5%

{1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron (114410-62-7) → {N(1)-(pyrid-2-yl)-N(2),N(3)-diphenylguanidinato}diisopropylboron (114410-63-8)

Guidance literature:

In neat (no solvent); 100-150°C, 2h;; washing with hexane, elem. anal.;

DOI:10.1007/BF00956368

Reference yield:

{1-(N,N'-diphenylamidino)pyridon-2-iminato}diisopropylboron (114410-62-7) → 2-diisopropylborylaminopyridine (114502-05-5) + 1,3-Diphenylcarbodiimide (622-16-2)

Guidance literature:

In neat (no solvent); decompn. between 70 and 90°C;

DOI:10.1007/BF00956368

upstream raw materials:

2-diisopropylborylaminopyridine

1,3-Diphenylcarbodiimide

Downstream raw materials:

2-diisopropylborylaminopyridine

1,3-Diphenylcarbodiimide

{N⁽¹⁾-(pyrid-2-yl)-N⁽²⁾,N⁽³⁾-diphenylguanidinato}diisopropylboron