9-cyclohexanyl>adenine

Base Information

Chemical Name:9-cyclohexanyl>adenine
CAS No.:162467-10-9
Molecular Formula:C₁₈H₃₀N₅O₄P
Molecular Weight:411.441
Hs Code.:

9-<cis-4'-<(Diisopropoxyphosphinyl)methoxy>cyclohexanyl>adenine

Synonyms:9-cyclohexanyl>adenine

Suppliers and Price of 9-cyclohexanyl>adenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-cyclohexanyl>adenine

Chemical Property:

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Technology Process of 9-cyclohexanyl>adenine

There total 8 articles about 9-cyclohexanyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(1R,4S)-4-(6-Azido-purin-9-yl)-cyclohex-2-enyloxymethyl]-phosphonic acid diisopropyl ester

: 162467-10-9
9-cyclohexanyl>adenine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 5h; Yield given; Ambient temperature;
DOI:10.1021/jo00111a010

Reference yield:

: 35717-98-7
bis(2-propyl)-p-toluenesulfonyloxymethylphosphonate

: 162467-10-9
9-cyclohexanyl>adenine

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / dimethylformamide / Ambient temperature

2: 80percent aq. AcOH / 0.5 h / 60 °C

3: 40 percent / Ph₃P, DEAD / dioxane / 2 h / Ambient temperature

4: NaN₃ / dimethylformamide / 3 h / 70 °C

5: H₂ / 10percent Pd/C / ethanol / 5 h / Ambient temperature

With sodium azide; hydrogen; sodium hydride; acetic acid; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00111a010

Reference yield:

: 41513-32-0
trans-2-cyclohexene-1,4-diol

: 162467-10-9
9-cyclohexanyl>adenine

Guidance literature:: Multi-step reaction with 6 steps

1: 51 percent / Et₃N, DMAP / CH₂Cl₂ / 48 h / Ambient temperature

2: NaH / dimethylformamide / Ambient temperature

3: 80percent aq. AcOH / 0.5 h / 60 °C

4: 40 percent / Ph₃P, DEAD / dioxane / 2 h / Ambient temperature

5: NaN₃ / dimethylformamide / 3 h / 70 °C

6: H₂ / 10percent Pd/C / ethanol / 5 h / Ambient temperature

With dmap; sodium azide; hydrogen; sodium hydride; acetic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00111a010