5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

Base Information

Chemical Name:5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone
CAS No.:1269998-96-0
Molecular Formula:C₂₂H₁₇N₃O₄
Molecular Weight:387.395
Hs Code.:

Synonyms:5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

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Chemical Property of 5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

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Technology Process of 5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

There total 5 articles about 5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1270000-64-0
3-oxo-1-cyclohexen-1-yl 1,6-dihydro-6-oxo-1-iphenyl-2-(3-pyridinyl)-5-pyrimidinecarboxylate

: 1269998-96-0
5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

Guidance literature:: With cesium fluoride; tetrabutylammomium bromide; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 62-53-3
aniline

: 1269998-96-0
5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 18 h / 10 - 20 °C

2.1: 8 h / 160 °C

3.1: pyridine; lithium iodide / 12 h / 125 - 130 °C

3.2: pH 7

4.1: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 20 °C

5.1: cesium fluoride / tetrabutylammomium bromide / acetonitrile / 3 h / 20 °C

With pyridine; 2-chloro-1-methyl-pyridinium iodide; sodium hydride; triethylamine; cesium fluoride; lithium iodide; tetrabutylammomium bromide; In dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;

Reference yield:

: 32622-22-3
N-phenylnicotinimidamide

: 1269998-96-0
5-((2-hydroxy-6-oxo-1-cyclohexen-1-yl)carbonyl)-3-phenyl-2-(3-pyridinyl)-4(3H)-pyrimidinone

Guidance literature:: Multi-step reaction with 4 steps

1.1: 8 h / 160 °C

2.1: pyridine; lithium iodide / 12 h / 125 - 130 °C

2.2: pH 7

3.1: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 20 °C

4.1: cesium fluoride / tetrabutylammomium bromide / acetonitrile / 3 h / 20 °C

With pyridine; 2-chloro-1-methyl-pyridinium iodide; triethylamine; cesium fluoride; lithium iodide; tetrabutylammomium bromide; In dichloromethane; acetonitrile;