(E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

Base Information

Chemical Name:(E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate
CAS No.:1360054-12-1
Molecular Formula:C₁₄H₁₆Cl₃NO₃
Molecular Weight:352.645
Hs Code.:

Synonyms:(E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

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Technology Process of (E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

There total 2 articles about (E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1360054-36-9
(E)-2-(5-hydroxypent-3-enyl)-4-methoxyphenol

: 545-06-2
trichloroacetonitrile

: 1360054-12-1
(E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

Guidance literature:: With sodium hydride; In diethyl ether; mineral oil; at 0 - 20 ℃; for 1.25h;
DOI:10.1021/jo202553a

Reference yield:

: 783333-02-8
(E)-5-(2-((tert-butyldimethylsilyl)oxy)-5-methoxyphenyl)pent-2-en-1-ol

: 1360054-12-1
(E)-5-(2-hydroxy-5-methoxyphenyl)pent-2-enyl 2,2,2-trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: sodium hydride / diethyl ether; mineral oil / 1.25 h / 0 - 20 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; diethyl ether; mineral oil;
DOI:10.1021/jo202553a