1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

Base Information

Chemical Name:1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine
CAS No.:133671-20-2
Molecular Formula:C₂₅H₂₉Cl₂N₃O₃
Molecular Weight:490.43
Hs Code.:

Synonyms:1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

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Chemical Property of 1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

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Technology Process of 1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

There total 5 articles about 1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 133671-15-5
1-(Carbobenzyloxy)-trans-4-(methylamino)-3-pyrrolidinylpiperidine

: 3024-72-4
3,4-dichlorobenzoyl chloride

: 133671-20-2
1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

Guidance literature:: With triethylamine; In diethyl ether;
DOI:10.1021/jo00009a038

Reference yield:

: 694-05-3
1,2,3,6-tetrahydropyridine

: 133671-20-2
1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 10percent aq. Na₂CO₃ / 2 h / 0 °C

2: 92 percent / m-CPBA / CH₂Cl₂ / 4 h / 0 deg C to r.t.

4: 90 percent / Et₃N / diethyl ether

With sodium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jo00009a038

Reference yield:

: 66207-08-7,1624258-63-4
3,4-epoxy-piperidine-1-carboxylic acid benzyl ester

: 133671-20-2
1-(Carbobenzyloxy)-trans-4-(N-methyl-3',4'-dichlorobenzamido)-3-pyrrolidinylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

2: 90 percent / Et₃N / diethyl ether

With triethylamine; In diethyl ether;
DOI:10.1021/jo00009a038