1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene

Base Information

• Chemical Name: 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene
• CAS No.: 171598-57-5
• Molecular Formula: C₁₅H₂₃BrO₃
• Molecular Weight: 331.25

Synonyms:1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene

Chemical Property of 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene

There total 2 articles about 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[4-((1S,2S,3R)-1,3-Dimethoxy-2-methoxymethyl-butyl)-phenyl]-methanol (196880-52-1) → 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene (171598-57-5)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1002/hlca.19970800522

Reference yield:

tert-Butyl-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-diphenyl-silane (196880-51-0) → 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene (171598-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / TBAF / tetrahydrofuran / 24 h / Ambient temperature

2: 78 percent / Br₄C, Ph₃P / tetrahydrofuran / 3 h / Ambient temperature

With carbon tetrabromide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;

DOI:10.1002/hlca.19970800522

Reference yield: 95.0%

(2R,3S,4R)-3-(hydroxymethyl)-5,5-dimethylhexane-2,4-diol (147673-38-9) + 1-Bromomethyl-4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzene (171598-57-5) → C54H86O12

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 4h; Heating;

DOI:10.1002/hlca.19970800522

upstream raw materials:

[4-((1S,2S,3R)-1,3-Dimethoxy-2-methoxymethyl-butyl)-phenyl]-methanol

tert-Butyl-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-diphenyl-silane

Downstream raw materials:

(4-{(1R,2S,3R)-1,3-Bis-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-benzyloxy)-tert-butyl-diphenyl-silane

(4-{(1S,2S,3R)-1,3-Bis-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-benzyloxy)-tert-butyl-diphenyl-silane

C₅₇H₈₃BrO₁₂

(4-{(1S,2S,3R)-1,3-Bis-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((1S,2S,3R)-1,3-dimethoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

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