C₄₉H₅₅N₃O₂*ClH

Base Information

Chemical Name:C₄₉H₅₅N₃O₂*ClH
CAS No.:1609262-63-6
Molecular Formula:C₄₉H₅₅N₃O₂*ClH
Molecular Weight:754.456
Hs Code.:

C<sub>49</sub>H<sub>55</sub>N<sub>3</sub>O<sub>2</sub>*ClH

Synonyms:C₄₉H₅₅N₃O₂*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₉H₅₅N₃O₂*ClH

Chemical Property:

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Technology Process of C₄₉H₅₅N₃O₂*ClH

There total 6 articles about C₄₉H₅₅N₃O₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1453873-66-9
C₃₅H₃₄N₂O₂S

: 2380-36-1
3,5-di-tert-butylaniline

: 1609262-63-6
C₄₉H₅₅N₃O₂*ClH

Guidance literature:: C₃₅H₃₄N₂O₂S; With potassium carbonate; copper(l) chloride; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

3,5-di-tert-butylaniline; at 40 ℃; for 48h;
DOI:10.1039/c4cc01817f

Reference yield:

: 61045-33-8,93922-63-5
diethyl (2R,3R)-1,4-dioxaspiro[4.5]decane-2,3-dicarboxylate

: 1609262-63-6
C₄₉H₅₅N₃O₂*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromobenzene; magnesium / tetrahydrofuran / 1.5 h / Reflux

2.1: thionyl chloride; triethylamine / dichloromethane / 3 h / Inert atmosphere; Reflux

2.2: 72 h / 80 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

4.1: pyridine / 7 h / 60 °C

5.1: copper(l) chloride; potassium carbonate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

5.2: 48 h / 40 °C

With lithium aluminium tetrahydride; thionyl chloride; bromobenzene; potassium carbonate; magnesium; triethylamine; copper(l) chloride; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1039/c4cc01817f

Reference yield:

: 1453873-64-7
C₃₄H₃₂N₆O₂

: 1609262-63-6
C₄₉H₅₅N₃O₂*ClH

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2.1: pyridine / 7 h / 60 °C

3.1: copper(l) chloride; potassium carbonate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3.2: 48 h / 40 °C

With lithium aluminium tetrahydride; potassium carbonate; copper(l) chloride; In tetrahydrofuran; pyridine;
DOI:10.1039/c4cc01817f