(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

Base Information

Chemical Name:(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate
CAS No.:161392-03-6
Molecular Formula:C₃₁H₃₈O₄S
Molecular Weight:506.706
Hs Code.:

Synonyms:(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

Chemical Property:

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Technology Process of (2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

There total 5 articles about (2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 161392-02-5
(2S)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl p-toluenesulfonate

: 10387-40-3
potassium thioacetate

: 161392-03-6
(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 16h;
DOI:10.1021/jm00050a009

Reference yield:

: 111-25-1
1-bromo-hexane

: 161392-03-6
(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) DMF, 45 min, 2.) DMF, 25 deg C, 14 h

2: 100 percent / 1 N HCl / methanol / 24 h / 25 °C

3: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

4: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

5: 70 percent / dimethylformamide / 16 h / 80 °C

With pyridine; hydrogenchloride; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: 86158-13-6
(2S)-3-(hexyloxy)-1,2-propanediol

: 161392-03-6
(2R)-1-(hexyloxy)-3-<(4-methoxyphenyl)diphenylmethoxy>-2-propyl thioacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

2: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

3: 70 percent / dimethylformamide / 16 h / 80 °C

With pyridine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009