C₁₃H₁₇ISi

Base Information

Chemical Name:C₁₃H₁₇ISi
CAS No.:1520097-25-9
Molecular Formula:C₁₃H₁₇ISi
Molecular Weight:328.268
Hs Code.:

Synonyms:C₁₃H₁₇ISi

Suppliers and Price of C₁₃H₁₇ISi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₇ISi

Chemical Property:

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Safty Information:

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Technology Process of C₁₃H₁₇ISi

There total 6 articles about C₁₃H₁₇ISi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1520097-25-9
C₁₃H₁₇ISi

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 2 h / 20 - 75 °C / 760.05 Torr / Inert atmosphere

1.2: 16 h / 20 - 75 °C / 760.05 Torr / Inert atmosphere

2.1: acetyl chloride; methanol / 3 h / 0 °C / 760.05 Torr / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / acetonitrile; diethyl ether / 1 h / 0 °C / 760.05 Torr / Inert atmosphere

With 1H-imidazole; methanol; ethylmagnesium bromide; iodine; acetyl chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.3762/bjoc.9.258

Reference yield:

: 1520097-16-8
C₁₉H₃₂OSi₂

: 1520097-25-9
C₁₃H₁₇ISi

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride; methanol / 3 h / 0 °C / 760.05 Torr / Inert atmosphere

2: 1H-imidazole; iodine; triphenylphosphine / acetonitrile; diethyl ether / 1 h / 0 °C / 760.05 Torr / Inert atmosphere

With 1H-imidazole; methanol; iodine; acetyl chloride; triphenylphosphine; In diethyl ether; acetonitrile;
DOI:10.3762/bjoc.9.258

Reference yield:

: 1025885-73-7
tert-Butyl-(2-iodomethyl-benzyloxy)-dimethyl-silane

: 1520097-25-9
C₁₃H₁₇ISi

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 2 h / 20 - 75 °C / 760.05 Torr / Inert atmosphere

1.2: 16 h / 20 - 75 °C / 760.05 Torr / Inert atmosphere

2.1: acetyl chloride; methanol / 3 h / 0 °C / 760.05 Torr / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / acetonitrile; diethyl ether / 1 h / 0 °C / 760.05 Torr / Inert atmosphere

With 1H-imidazole; methanol; ethylmagnesium bromide; iodine; acetyl chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.3762/bjoc.9.258