4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

Base Information

Chemical Name:4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide
CAS No.:1308255-23-3
Molecular Formula:C₁₇H₂₁BN₄O₅S
Molecular Weight:404.255
Hs Code.:

Synonyms:4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

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Chemical Property of 4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

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Technology Process of 4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

There total 5 articles about 4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1308254-86-5
4-amino-2-(aminomethyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

: 76-05-1
trifluoroacetic acid

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1308255-23-3
4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

: 1308255-24-4
N-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzyl)-2,2,2-trifluoroacetamide

Guidance literature:: 4-amino-2-(aminomethyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide; N,N-Dimethylcarbamoyl chloride; With pyridine; at 20 ℃; for 16h;

trifluoroacetic acid;

Reference yield:

: 16588-02-6
4-chloro-3-cyanonitrobenzene

: 1308255-23-3
4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 20 °C

2: acetic acid; chlorine / water / 2 h / 15 °C

3: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

4: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

5: pyridine / 16 h / 20 °C

With 4-methyl-morpholine; pyridine; ammonium hydroxide; hydrogen; chlorine; potassium carbonate; acetic acid; In methanol; water; acetonitrile;

Reference yield:

: 175135-67-8
2-(benzylthio)-5-nitrobenzonitrile

: 1308255-23-3
4-amino-2-((3,3-dimethylureido)methyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; chlorine / water / 2 h / 15 °C

2: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

3: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

4: pyridine / 16 h / 20 °C

With 4-methyl-morpholine; pyridine; ammonium hydroxide; hydrogen; chlorine; acetic acid; In methanol; water; acetonitrile;