(hexacarbonyldicobalt)propargyl para-fluorophenyl ether

Base Information

Chemical Name:(hexacarbonyldicobalt)propargyl para-fluorophenyl ether
CAS No.:1417919-55-1
Molecular Formula:C₁₅H₇Co₂FO₇
Molecular Weight:436.201
Hs Code.:

Synonyms:(hexacarbonyldicobalt)propargyl para-fluorophenyl ether

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Chemical Property of (hexacarbonyldicobalt)propargyl para-fluorophenyl ether

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Technology Process of (hexacarbonyldicobalt)propargyl para-fluorophenyl ether

There total 2 articles about (hexacarbonyldicobalt)propargyl para-fluorophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 124700-26-1
1-fluoro-4-(2-propynyloxy)benzene

: 1417919-55-1
(hexacarbonyldicobalt)propargyl para-fluorophenyl ether

Guidance literature:: In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.jinorgbio.2012.10.014

Reference yield:

: 371-41-5
4-Fluorophenol

: 1417919-55-1
(hexacarbonyldicobalt)propargyl para-fluorophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 55 °C

1.2: 4 h / 20 °C

2.1: tetrahydrofuran / 20 °C / Inert atmosphere

With potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.jinorgbio.2012.10.014