Technology Process of C19H23NO5
There total 6 articles about C19H23NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H29NO6;
With
hydrogenchloride; water;
In
tetrahydrofuran; methanol;
for 24h;
With
sodium hydroxide;
In
tetrahydrofuran; methanol; water;
at 60 ℃;
for 6h;
Further stages;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide; potassium carbonate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / 21.5 h / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethanol / 17.5 h / Inert atmosphere
4.1: caesium carbonate / acetonitrile / 15.5 h
5.1: hydrogenchloride; water / tetrahydrofuran; methanol / 24 h
5.2: 6 h / 60 °C
With
hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; water; hydrogen; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium 10% on activated carbon; hydrogen / ethanol / 17.5 h / Inert atmosphere
2.1: caesium carbonate / acetonitrile / 15.5 h
3.1: hydrogenchloride; water / tetrahydrofuran; methanol / 24 h
3.2: 6 h / 60 °C
With
hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; caesium carbonate;
In
tetrahydrofuran; methanol; ethanol; acetonitrile;
