(+)-8,9-dihydrobenzanthracene 10,11-oxide

Base Information

• Chemical Name: (+)-8,9-dihydrobenz
• Molecular Formula: C₁₈H₁₄O
• Molecular Weight: 246.309

Synonyms:(+)-8,9-dihydrobenzanthracene 10,11-oxide

Chemical Property of (+)-8,9-dihydrobenz

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

There total 1 articles about (+)-8,9-dihydrobenzanthracene 10,11-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride (39637-99-5,20445-33-4) → (+)-8,9-dihydrobenzanthracene 10,11-oxide (79252-29-2)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

2: N-bromosuccinimide

3: NaOMe / tetrahydrofuran

With N-Bromosuccinimide; sodium methylate; In tetrahydrofuran; pyridine;

DOI:10.1016/S0040-4039(01)81884-0

Reference yield:

(+)-8,9-dihydrobenzanthracene 10,11-oxide (79252-29-2) → (+)-10-benzoyloxy-8,9,10,11-tetrahydrobenzanthracene (79252-27-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / LiAlH₄ / diethyl ether

2: 65 percent / pyridine

With pyridine; lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1039/P19810002233

upstream raw materials:

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

Downstream raw materials:

(+)-10-benzoyloxy-8,9,10,11-tetrahydrobenzanthracene

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