5-(4-methoxybenzylthio)-8-nitroisoquinoline

Base Information

Chemical Name:5-(4-methoxybenzylthio)-8-nitroisoquinoline
CAS No.:1602769-95-8
Molecular Formula:C₁₇H₁₄N₂O₃S
Molecular Weight:326.376
Hs Code.:

Synonyms:5-(4-methoxybenzylthio)-8-nitroisoquinoline

Suppliers and Price of 5-(4-methoxybenzylthio)-8-nitroisoquinoline

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Chemical Property of 5-(4-methoxybenzylthio)-8-nitroisoquinoline

Chemical Property:

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Technology Process of 5-(4-methoxybenzylthio)-8-nitroisoquinoline

There total 3 articles about 5-(4-methoxybenzylthio)-8-nitroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 63927-23-1
5-bromo-8-nitroisoquinoline

: 6258-60-2
p-methoxybenzylmercaptan

: 1602769-95-8
5-(4-methoxybenzylthio)-8-nitroisoquinoline

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1002/cmdc.201300378

Reference yield:

: 119-65-3
isoquinoline

: 1602769-95-8
5-(4-methoxybenzylthio)-8-nitroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; N-Bromosuccinimide / 5 h / -26 - 30 °C / Inert atmosphere; Cooling with acetone-dry ice

2: potassium nitrate / 1 h / -10 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 130 °C / Microwave irradiation

With N-Bromosuccinimide; sulfuric acid; potassium carbonate; potassium nitrate; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201300378

Reference yield:

: 34784-04-8
5-bromoisoquinoline

: 1602769-95-8
5-(4-methoxybenzylthio)-8-nitroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium nitrate / 1 h / -10 °C

2: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 130 °C / Microwave irradiation

With potassium carbonate; potassium nitrate; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201300378