4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

Base Information

Chemical Name:4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide
CAS No.:1353687-20-3
Molecular Formula:C₃₅H₄₇NOSi₂
Molecular Weight:553.935
Hs Code.:

Synonyms:4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

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Chemical Property of 4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

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Technology Process of 4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

There total 5 articles about 4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1353687-17-8
N-decyl-4-ethynylbenzamide

: 144001-09-2
(5-bromo-1,3-phenylene)bis(ethyne-2,1-diyl)bis(trimethylsilane)

: 1353687-20-3
4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 70 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja210443m

Reference yield:

: 1353687-16-7
N-decyl-4-(2-(trimethylsilyl)ethynyl)benzamide

: 1353687-20-3
4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; methanol

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 24 h / 70 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; 2: Sonogashira coupling;
DOI:10.1021/ja210443m

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 1353687-20-3
4-(2-(3,5-bis(2-(trimethylsilyl)ethynyl)phenyl)ethynyl)-N-decylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 24 h / 70 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; 1: Sonogashira coupling / 2: Sonogashira coupling;
DOI:10.1021/ja210443m