3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
CAS No.:951402-58-7
Molecular Formula:C₂₃H₁₉BF₂N₂O
Molecular Weight:388.224
Hs Code.:

Synonyms:3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 877616-00-7
3-methoxy-5-chloro-4,4-difluoro-4-bora-8-(4-methylphenyl)-3a,4a-diaza-s-indacene

: 98-80-6
phenylboronic acid

: 951402-58-7
3-methoxy-5-phenyl-8-(4-tolyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With Na₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; other Radiation; to soln. of (CH3C6H4)C9H4N2BF2Cl(OCH3) in DME added PhB(OH)2, Na2CO3 andcatalytic amount of Pd(PPh3)4, mixt. stirred under MW irradn. for 20 mi n at 150 °C and 200 W; quenched (H2O), extrd. (CH2Cl2), dried (MgSO4), evapd. under reduced pressure, chromy. on silica gel (CH2Cl2);
DOI:10.1021/jp073547+