[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide

Base Information

• Chemical Name: [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide
• CAS No.: 111828-14-9
• Molecular Formula: C₁₁H₁₄N₆O₂S
• Molecular Weight: 294.337

Synonyms:[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide

Chemical Property of [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide

Chemical Property:

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Technology Process of [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide

There total 3 articles about [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid methyl ester (111828-09-2) → [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide (111828-14-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Heating;

DOI:10.1002/jhet.5570230540

Reference yield:

potassium N-(4-methoxybenzoyl)hydrazinecarbodithioate (85103-41-9) → [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide (111828-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 59 percent / Hydrazine hydrate / H₂O / 1 h / Heating

2: 85 percent / 1) Sodium hydroxide / ethanol / 1) Reflux 0.5 h, 2) reflux 4 h.

3: 79 percent / Hydrazine hydrate / ethanol / 2 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol; water;

DOI:10.1002/jhet.5570230540

Reference yield:

4-amino-5-(4-methoxyphenyl)-4H-1,2,4-triazole-3-thiol (36209-49-1) → [4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid hydrazide (111828-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 1) Sodium hydroxide / ethanol / 1) Reflux 0.5 h, 2) reflux 4 h.

2: 79 percent / Hydrazine hydrate / ethanol / 2 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;

DOI:10.1002/jhet.5570230540

upstream raw materials:

[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid methyl ester

potassium N-(4-methoxybenzoyl)hydrazinecarbodithioate

4-amino-5-(4-methoxyphenyl)-4H-1,2,4-triazole-3-thiol

Downstream raw materials:

[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

[4-Amino-5-(4-methoxy-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-acetic acid [1-(4-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

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