(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

Base Information

Chemical Name:(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide
CAS No.:1446203-43-5
Molecular Formula:C₁₉H₁₂ClNO₂
Molecular Weight:321.763
Hs Code.:

Synonyms:(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

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Chemical Property of (2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

Chemical Property:

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Technology Process of (2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

There total 4 articles about (2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1446203-31-1
3-(4-chlorophenyl)-N-(4-hydroxynaphthalen-1-yl)acrylamide

: 1446203-43-5
(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

Guidance literature:: With sodium periodate; silica gel; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2013.03.043

Reference yield:

: 605-62-9
4-nitro-1-naphthol

: 1446203-43-5
(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / methanol / 12 h

2: sodium hydrogencarbonate / water; tetrahydrofuran / 5 h / 20 °C / Cooling with ice

3: sodium periodate; silica gel / dichloromethane / 2 h / 20 °C

With sodium periodate; palladium on activated charcoal; hydrogen; silica gel; sodium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2013.03.043

Reference yield:

: 86-57-7
1-Nitronaphthalene

: 1446203-43-5
(2E,NE)-3-(4-chlorophenyl)-N-(4-oxonaphthalen-1(4H)-ylidene)acrylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / dimethyl sulfoxide; water / 0.08 h / 0 - 5 °C

1.2: 2 h / 20 °C

2.1: hydrogen; palladium on activated charcoal / methanol / 12 h

3.1: sodium hydrogencarbonate / water; tetrahydrofuran / 5 h / 20 °C / Cooling with ice

4.1: sodium periodate; silica gel / dichloromethane / 2 h / 20 °C

With sodium periodate; palladium on activated charcoal; hydrogen; silica gel; sodium hydrogencarbonate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2013.03.043