2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

Base Information

Chemical Name:2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine
CAS No.:135968-95-5
Molecular Formula:C₃₃H₄₈N₂O₁₁
Molecular Weight:648.751
Hs Code.:

Synonyms:2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

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Technology Process of 2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

There total 3 articles about 2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 108342-87-6
tetra-O-pivaloyl-β-D-galactopyranosylamine

: 552-89-6
2-nitro-benzaldehyde

: 135968-95-5
2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

Guidance literature:: With acetic acid;

Reference yield:

: 108342-86-5
2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl azide

: 135968-95-5
2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂

2: glacial acetic acid / propan-2-ol

With hydrogen; acetic acid; In isopropyl alcohol;

Reference yield:

: 108342-85-4,118711-42-5,220017-47-0
1,2,3,4,6-penta-O-pivaloyl-β-D-galactopyranose

: 135968-95-5
2-nitro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / trimethylsilyl azide, SnCl₄ / CH₂Cl₂ / 5 h

2: 87 percent / H₂ / Raney nickel / methanol / 3 h / 760 Torr

3: 86 percent / HOAc

With trimethylsilylazide; hydrogen; tin(IV) chloride; acetic acid; nickel; In methanol; dichloromethane;