5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

Base Information

Chemical Name:5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole
CAS No.:109855-80-3
Molecular Formula:C₁₇H₁₄N₂
Molecular Weight:246.312
Hs Code.:

Synonyms:5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

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Chemical Property of 5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

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Technology Process of 5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

There total 7 articles about 5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109855-79-0
7-(2-azidophenyl)-5,8-dimethylisoquinoline

: 519-23-3
ellipticine

: 109855-80-3
5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

Guidance literature:: In dodecane; at 180 - 200 ℃;

Reference yield:

: 119-65-3
isoquinoline

: 519-23-3
ellipticine

: 109855-80-3
5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid; trichloroisocyanuric acid / 0 - 25 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; toluene / 85 °C / Schlenk technique; Inert atmosphere

3.1: sulfuric acid; N-Bromosuccinimide / 6 h / 0 - 25 °C

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dichloro-ethane / 85 °C / Schlenk technique; Inert atmosphere

5.1: sulfuric acid; water / ethanol / 24 h / 120 °C

6.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C

6.2: 1 h / 0 - 5 °C

7.1: 1,2-dichloro-benzene / 1 h / 190 °C / Microwave irradiation

With hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trichloroisocyanuric acid; sulfuric acid; water; sodium carbonate; sodium nitrite; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; 1,2-dichloro-benzene; toluene; 4.1: |Suzuki Coupling;
DOI:10.1055/s-0037-1609153

Reference yield:

: 73075-59-9
5,8-dichloroisoquinoline

: 519-23-3
ellipticine

: 109855-80-3
5,6a-dimethyl-6aH-pyrido[3,4-a]carbazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; toluene / 85 °C / Schlenk technique; Inert atmosphere

2.1: sulfuric acid; N-Bromosuccinimide / 6 h / 0 - 25 °C

3.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dichloro-ethane / 85 °C / Schlenk technique; Inert atmosphere

4.1: sulfuric acid; water / ethanol / 24 h / 120 °C

5.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C

5.2: 1 h / 0 - 5 °C

6.1: 1,2-dichloro-benzene / 1 h / 190 °C / Microwave irradiation

With hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; water; sodium carbonate; sodium nitrite; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; 1,2-dichloro-benzene; toluene; 3.1: |Suzuki Coupling;
DOI:10.1055/s-0037-1609153