t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine

Base Information

• Chemical Name: t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine
• CAS No.: 1363676-12-3
• Molecular Formula: C₃₉H₄₁N₇O₆
• Molecular Weight: 703.798

Synonyms:t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine

Chemical Property of t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine

Chemical Property:

Purity/Quality:

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Technology Process of t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine

There total 1 articles about t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-vinyl-guanin-9-yl]glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O6-benzyl-8-bromo-guanin-9-yl]glycine (1363676-09-8) + tri-n-butyl(vinyl)tin (7486-35-3) → t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O6-benzyl-8-vinyl-guanin-9-yl]glycine (1363676-12-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1-methyl-pyrrolidin-2-one; at 70 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ol3000603

upstream raw materials:

t-butyl-N-[2-(fluorenylmethoxycarbonyl)aminoethyl]-N-[O₆-benzyl-8-bromo-guanin-9-yl]glycine

tri-n-butyl(vinyl)tin

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