(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

Base Information

Chemical Name:(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran
CAS No.:894358-66-8
Molecular Formula:C₃₅H₃₈O₅S₂
Molecular Weight:602.816
Hs Code.:

Synonyms:(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

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Chemical Property of (2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

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Technology Process of (2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

There total 1 articles about (2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 72174-24-4
2,3,4,6-tetra-O-benzyl-1-thio-α/β-D-glucopyranose

: 85055-60-3
dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate

: 894358-66-8
(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2006.03.104

Reference yield: 82.0%

: 894358-66-8
(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

: 894358-67-9
C₃₅H₃₈O₆S₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1016/j.tetlet.2006.03.104

Reference yield:

: 894358-66-8
(2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyldisulfanyl-tetrahydro-pyran

: 118206-39-6
2,3,4,6-tetra-O-benzyl-D-glucono-δ-thionolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / MCPBA / CH₂Cl₂ / 0 °C

2: 63 percent / 4 Angstroem molecular sieves / toluene / 0.25 h / 120 °C

With 4 A molecular sieve; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2006.03.104