(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

Base Information

Chemical Name:(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide
CAS No.:244203-13-2
Molecular Formula:C₂₂H₃₄BrNO₂
Molecular Weight:424.421
Hs Code.:

Synonyms:(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

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Chemical Property of (1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

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Technology Process of (1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

There total 2 articles about (1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 244203-12-1
(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carbonyl chloride

: 244203-13-2
(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1248/cpb.47.909

Reference yield:

: (+)-3α-bromocamphor

: 244203-13-2
(1S,3S,4S)-3-Bromo-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid dicyclohexylamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃ / 2 h / Heating

2: 31 percent / Et₃N / CH₂Cl₂ / 13 h / 0 - 20 °C

With thionyl chloride; triethylamine; In dichloromethane; chloroform; 1: Substitution / 2: Condensation;
DOI:10.1023/A:1009511802235