(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

Base Information

Chemical Name:(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid
CAS No.:1027640-30-7
Molecular Formula:C₂₈H₅₁NO₈Si₂
Molecular Weight:585.886
Hs Code.:

(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

Synonyms:(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

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Chemical Property of (3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

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Technology Process of (3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

There total 1 articles about (3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85781-30-2
{(1R,2R)-1-[(1S,2S)-3-(tert-Butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-hydroxy-propyl]-2-hydroxy-pent-4-enyl}-carbamic acid benzyl ester

: 1027640-30-7
(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

Guidance literature:: With potassium permanganate; sodium periodate; potassium carbonate; In water; tert-butyl alcohol; for 15h;
DOI:10.1021/ja00350a061

Reference yield:

: 1027640-30-7
(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dihydroxy-heptanoic acid

: 85781-31-3
(3R,4R,5S,6S)-4-Benzyloxycarbonylamino-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-bis-methoxymethoxy-heptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0.5 h

2: i-Pr₂EtN / CHCl₃ / 5 h / 60 °C

With N-ethyl-N,N-diisopropylamine; In diethyl ether; chloroform;
DOI:10.1021/ja00350a061