1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate

Base Information

• Chemical Name: 1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate
• CAS No.: 1300116-27-1
• Molecular Formula: CF₃O₃S*C₃₃H₃₅O₃S
• Molecular Weight: 660.776

Synonyms:1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate

Chemical Property of 1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate

There total 1 articles about 1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1,4-anhydro-2,3,5-tri-O-benzyl-4-thio-D-arabinitol (187590-77-8) + benzyl 2,3,4-tri-O-benzyl-6-O-trifluoromethanesulfonyl-α-D-mannopyranoside → benzyl 2,4-di-O-benzyl-3,6-anhydro-α-D-mannopyranoside (1300116-25-9) + 1,4-dideoxy-1,4-[(R)-benzylepisulfoniumylidene]-D-arabinitol trifluoromethanesulfonate (1300116-27-1) + 2,3,5-tri-O-benzyl-1,4-dideoxy-1,4-[(S)-(1,2,3,4-tetra-O-benzyl-6-deoxy-α-D-mannopyranos-6-yl)episulfoniumylidene]-D-arabinitol trifluoromethanesulfonate (1300116-24-8)

Guidance literature:

In tetrahydrofuran; at 0 ℃; for 17h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.01.052

upstream raw materials:

1,4-anhydro-2,3,5-tri-O-benzyl-4-thio-D-arabinitol

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