C₂₈H₃₄ClN₇O₅S

Base Information

Chemical Name:C₂₈H₃₄ClN₇O₅S
CAS No.:1353625-24-7
Molecular Formula:C₂₈H₃₄ClN₇O₅S
Molecular Weight:616.141
Hs Code.:

C<sub>28</sub>H<sub>34</sub>ClN<sub>7</sub>O<sub>5</sub>S

Synonyms:C₂₈H₃₄ClN₇O₅S

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Chemical Property of C₂₈H₃₄ClN₇O₅S

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Technology Process of C₂₈H₃₄ClN₇O₅S

There total 9 articles about C₂₈H₃₄ClN₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: (x)C₂HF₃O₂*C₂₃H₂₇ClN₆O₄S

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 1353625-24-7
C₂₈H₃₄ClN₇O₅S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 3h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353625-24-7
C₂₈H₃₄ClN₇O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: caesium carbonate / 17 h / 130 °C

5.1: trichlorophosphate / 2 h / 100 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 70 °C

8.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h

With dmap; sodium bis(trimethylsilyl)amide; hydrazinium monoacetate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In tetrahydrofuran; hexanes; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353625-24-7
C₂₈H₃₄ClN₇O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: caesium carbonate / 17 h / 130 °C

4.1: trichlorophosphate / 2 h / 100 °C

5.1: HATU / N,N-dimethyl-formamide / 1 h

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 70 °C

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h

With dmap; sodium bis(trimethylsilyl)amide; hydrazinium monoacetate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;