C₂₁H₃₆O

Base Information

Chemical Name:C₂₁H₃₆O
CAS No.:1263786-18-0
Molecular Formula:C₂₁H₃₆O
Molecular Weight:304.516
Hs Code.:

Synonyms:C₂₁H₃₆O

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Chemical Property of C₂₁H₃₆O

Chemical Property:

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Technology Process of C₂₁H₃₆O

There total 4 articles about C₂₁H₃₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1263786-16-8
C₂₃H₃₈O₂

: 1263786-18-0
C₂₁H₃₆O

Guidance literature:: With ammonia; In methanol; at 40 - 45 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo102188q

Reference yield:

: 108104-21-8
(S)-1-cyclohexyl-2-propyn-1-ol acetate

: 1263786-18-0
C₂₁H₃₆O

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine / 0.5 h / 20 °C

1.2: 1.5 h / 20 °C

2.1: ammonia / methanol / 2 h / 40 - 45 °C / Inert atmosphere

With copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; ammonia; triethylamine; In methanol; 1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1021/jo102188q

Reference yield:

: 906533-64-0
(S)-1-cyclohexyl-3-(triethylsilyl)prop-2-yn-1-ol

: 1263786-18-0
C₂₁H₃₆O

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

2.1: pyridine / 48 h / 25 °C

3.1: copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine / 0.5 h / 20 °C

3.2: 1.5 h / 20 °C

4.1: ammonia / methanol / 2 h / 40 - 45 °C / Inert atmosphere

With pyridine; copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; tetrabutyl ammonium fluoride; ammonia; triethylamine; In tetrahydrofuran; methanol; 3.1: Sonogashira coupling / 3.2: Sonogashira coupling;
DOI:10.1021/jo102188q