9,10-Dichlorooctafluoroanthracene

Base Information

Chemical Name:9,10-Dichlorooctafluoroanthracene
CAS No.:219724-46-6
Molecular Formula:C₁₄Cl₂F₈
Molecular Weight:391.047
Hs Code.:
European Community (EC) Number:694-434-3
Nikkaji Number:J2.505.256K
Mol file:219724-46-6.mol

Synonyms:9,10-dichlorooctafluoroanthracene;219724-46-6;9,10-dichloro-1,2,3,4,5,6,7,8-octafluoroanthracene;SCHEMBL8372685;9,10-Dichlorooctafluoroanthracene, 97%;9, 10-dichloro-1, 2, 3, 4, 5, 6, 7, 8-octafluoroanthracene

Suppliers and Price of 9,10-Dichlorooctafluoroanthracene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
9,10-Dichlorooctafluoroanthracene 97%
500mg
$ 147.00

Total 4 raw suppliers

Chemical Property of 9,10-Dichlorooctafluoroanthracene

Chemical Property:

Melting Point:166-173 °C
XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:0
Exact Mass:389.9249307
Heavy Atom Count:24
Complexity:402

Purity/Quality:

98%,99%, ^*data from raw suppliers

9,10-Dichlorooctafluoroanthracene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi,N
Statements: 36/37/38-50/53
Safety Statements: 26-60-61

MSDS Files:

Useful:

Canonical SMILES:C12=C(C(=C(C(=C1F)F)F)F)C(=C3C(=C2Cl)C(=C(C(=C3F)F)F)F)Cl
Uses 9,10-Dichlorooctafluoroanthracene can be used in the synthesis of n-type Organic Semiconductors. Used in the synthesis of n-type Organic Semiconductors.

Technology Process of 9,10-Dichlorooctafluoroanthracene

There total 5 articles about 9,10-Dichlorooctafluoroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 219710-93-7
9,9,10,10-tetrachlorooctafluoro-9,10-dihydroanthracene

: 219724-46-6
9,10-dichloro-1,2,3,4,5,6,7,8-octafluoroanthracene

Guidance literature:: With acetic acid; In 1-methyl-pyrrolidin-2-one; at 115 ℃; for 24h;
DOI:10.1021/jo070404a

Reference yield:

: 219710-93-7
9,9,10,10-tetrachlorooctafluoro-9,10-dihydroanthracene

: 9-chloro-1,2,3,4,5,6,7,8-octafluoroanthracene

: 219724-46-6
9,10-dichloro-1,2,3,4,5,6,7,8-octafluoroanthracene

: 56777-03-8
1,2,3,4,5,6,7,8-octafluoroanthracene

Guidance literature:: With zinc(II) chloride; zinc; In methanol; at 25 ℃; Title compound not separated from byproducts.;
DOI:10.1021/jo070404a

Reference yield:

: 652-12-0
4,5,6,7-tetrafluoroisobenzofuran-1,3-dione

: 219724-46-6
9,10-dichloro-1,2,3,4,5,6,7,8-octafluoroanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / CsF / m-xylene; tetrahydrothiophene 1,1-dioxide / 0.5 h / 160 °C

2: 83 percent / PCl₅; phenylphosphonic dichloride / 26 h / 130 - 170 °C

3: 85 percent / glacial AcOH / 1-methyl-pyrrolidin-2-one / 24 h / 115 °C

With P,P-dichlorophenylphosphine oxide; phosphorus pentachloride; acetic acid; cesium fluoride; In 1-methyl-pyrrolidin-2-one; sulfolane; m-xylene;
DOI:10.1021/jo070404a