2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde

Base Information

• Chemical Name: 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde
• CAS No.: 132938-17-1
• Molecular Formula: C₄₆H₄₈N₄O
• Molecular Weight: 672.913

Synonyms:2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde

Chemical Property of 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde

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Technology Process of 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde

There total 5 articles about 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5Z,10Z,14Z,19Z)-5-[2-(5,5-Dimethyl-[1,3]dioxan-2-yl)-phenyl]-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin → 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde (132938-17-1)

Guidance literature:

With sulfuric acid; trifluoroacetic acid; In dichloromethane; Yield given; Heating;

DOI:10.1021/ja00064a021

Reference yield:

bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane (92415-30-0) → 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde (132938-17-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) trichloroacetic acid, 2.) p-chloranil / 1.) CH₃CN, 16 h, 2.) CH₃CN, 3 h

2: CF₃COOH, aq. 10percent H₂SO₄ / CH₂Cl₂ / Heating

With sulfuric acid; chloranil; trifluoroacetic acid; trichloroacetic acid; In dichloromethane;

DOI:10.1021/ja00064a021

Reference yield:

4-methyl-benzaldehyde (104-87-0) → 2-((5Z,10Z,14Z,19Z)-2,8,12,18-Tetraethyl-3,7,13,17-tetramethyl-15-p-tolyl-porphyrin-5-yl)-benzaldehyde (132938-17-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) trichloroacetic acid, 2.) p-chloranil / 1.) CH₃CN, 16 h, 2.) CH₃CN, 3 h

2: CF₃COOH, aq. 10percent H₂SO₄ / CH₂Cl₂ / Heating

With sulfuric acid; chloranil; trifluoroacetic acid; trichloroacetic acid; In dichloromethane;

DOI:10.1021/ja00064a021

upstream raw materials:

bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

4-methyl-benzaldehyde

2-(5,5-dimethyl-1,3-dioxacyclohex-2-yl)benzaldehyde

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