Dibenzylamine hydrobromide

Base Information

• Chemical Name: Dibenzylamine hydrobromide
• CAS No.: 88358-66-1
• Molecular Formula: Br*C₁₄H₁₆N
• Molecular Weight: 278.192
• Hs Code.: 2921499090
• NSC Number: 150226
• Mol file: 88358-66-1.mol

Synonyms:dibenzylamine hydrobromide;88358-66-1;N,N-Dibenzylamine hydrobromide;SCHEMBL998627;WZBCIFZVBDLSDN-UHFFFAOYSA-N;NSC150226;AKOS003747876;NSC-150226;FT-0629440

Chemical Property of Dibenzylamine hydrobromide

Chemical Property:

• PSA: 12.03000
• LogP: 4.32540
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 277.04661
• Heavy Atom Count: 16
• Complexity: 137

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CNCC2=CC=CC=C2.Br

Technology Process of Dibenzylamine hydrobromide

There total 4 articles about Dibenzylamine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl Bromopyruvate (70-23-5) + dibenzylamine (103-49-1) → dibenzylamine hydrobromide (88358-66-1) + (Z)-3-Dibenzylamino-2-hydroxy-acrylic acid ethyl ester

Guidance literature:

In butanone; for 0.75h; Heating;

DOI:10.1002/jhet.5570210313

Reference yield:

1-ethyl-2-bromo-pyridinium; bromide (79343-93-4) + dibenzylamine (103-49-1) → dibenzylamine hydrobromide (88358-66-1) + 2-Dibenzylamino-1-ethyl-pyridinium; bromide

Guidance literature:

In acetonitrile; at 25 ℃; Rate constant; Product distribution; Mechanism; the effect of steric and electronic structure of the amine;

Reference yield:

→ dibenzylamine hydrobromide (88358-66-1)

Guidance literature:

upstream raw materials:

ethyl Bromopyruvate

dibenzylamine

1-ethyl-2-bromo-pyridinium; bromide

Refernces

• 1、 -. "Prostaglandins". . . Retrieved 2008/06/13.
• 2、 Litvinenko, L. M.,Titskii, G. D.,Mitchenko, E. S.. "KINETICS OF THE REACTIONS OF 2-HALOGENOPYRIDINIUM SALTS WITH PRIMARY AND SECONDARY AMINES IN ACETONITRILE". . p. 1731 - 1736. Retrieved 2007/10/02.