but-2-yn-1-yl 4-methylbenzoate

Base Information

• Chemical Name: but-2-yn-1-yl 4-methylbenzoate
• CAS No.: 913476-73-0
• Molecular Formula: C₁₂H₁₂O₂
• Molecular Weight: 188.226

Synonyms:but-2-yn-1-yl 4-methylbenzoate

Chemical Property of but-2-yn-1-yl 4-methylbenzoate

Chemical Property:

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Technology Process of but-2-yn-1-yl 4-methylbenzoate

There total 1 articles about but-2-yn-1-yl 4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methyl propargyl alcohol (764-01-2) + 4-methyl-benzoyl chloride (874-60-2) → but-2-yn-1-yl 4-methylbenzoate (913476-73-0)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/c4cc01370k

Reference yield: 41.0%

but-2-yn-1-yl 4-methylbenzoate (913476-73-0) + tris(pentafluorophenyl)borate (1109-15-5) → C30H12BF15O2 (1616403-15-6)

Guidance literature:

In toluene; at 20 ℃; for 96h; Inert atmosphere;

DOI:10.1039/c4cc01370k

upstream raw materials:

methyl propargyl alcohol

4-methyl-benzoyl chloride

Downstream raw materials:

C₃₀H₁₂BF₁₅O₂

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