(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

Base Information

Chemical Name:(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride
CAS No.:100230-98-6
Molecular Formula:C₂₀H₁₉ClN₂O₅
Molecular Weight:402.834
Hs Code.:

Synonyms:(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

Chemical Property:

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Technology Process of (S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

There total 2 articles about (S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18944-44-0
(2S)-N-<3-(benzyloxy)-4-methyl-2-nitrobenzoyl>proline

: 100230-98-6
(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In benzene; for 3h;
DOI:10.1021/jo00355a022

Reference yield:

: 6623-31-0
2-nitro-3-benzyloxy-4-methylbenzoic acid N-hydroxysuccinimide ester

: 100230-98-6
(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMF / benzene / 3 h

2: Et₃N / tetrahydrofuran; H₂O / 1 h / Ambient temperature

3: oxalyl chloride, DMF / benzene / 3 h

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; water; benzene;
DOI:10.1021/jo00355a022

Reference yield:

: 100230-98-6
(S)-1-(3-Benzyloxy-4-methyl-2-nitro-benzoyl)-pyrrolidine-2-carbonyl chloride

: 100230-82-8
N-<3-(benzyloxy)-4-methyl-2-nitrobenzoyl>pyrrolidine-2-carboxaldehyde

Guidance literature:: With bis(triphenylphosphine) copper borohydride; triphenylphosphine; In acetone; at 0 ℃; for 0.5h;
DOI:10.1021/jo00355a022