1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

Base Information

Chemical Name:1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane
CAS No.:104885-41-8
Molecular Formula:C₁₈H₁₂Cl₂N₆O₂S₂
Molecular Weight:479.37
Hs Code.:

Synonyms:1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

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Chemical Property of 1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

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Technology Process of 1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

There total 4 articles about 1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 104885-40-7
2-(p-chloroanilino)-1,3,4-thiadiazole-5-carboxaldehyde

: 104885-41-8
1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

Guidance literature:: With potassium cyanide; In ethanol; water; Ambient temperature;

Reference yield:

: 22814-92-2
4-(p-chlorophenyl)-3-thiosemicarbazide

: 104885-41-8
1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / ethanol; H₂O / 1 h / Heating

2: 80 percent / ferric chloride / ethanol / 0.17 h / Heating

3: 66 percent / sodium metaperiodate / H₂O / 2 h / Ambient temperature

4: 80 percent / aq. potassium cyanide / ethanol; H₂O / Ambient temperature

With potassium cyanide; sodium periodate; iron(III) chloride; In ethanol; water;

Reference yield:

: 104885-37-2
D-galactose 4-(p-chlorophenyl)thiosemicarbazone

: 104885-41-8
1,2-Di-<2-(p-chloroanilino)-1,3,4-thiadiazol-5-yl>-1-hydroxy-2-oxoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / ferric chloride / ethanol / 0.17 h / Heating

2: 66 percent / sodium metaperiodate / H₂O / 2 h / Ambient temperature

3: 80 percent / aq. potassium cyanide / ethanol; H₂O / Ambient temperature

With potassium cyanide; sodium periodate; iron(III) chloride; In ethanol; water;