1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

Base Information

Chemical Name:1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide
CAS No.:1191067-77-2
Molecular Formula:C₂₉H₂₆ClN₃O₃S
Molecular Weight:532.063
Hs Code.:

Synonyms:1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

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Chemical Property of 1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

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Technology Process of 1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

There total 3 articles about 1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 63201-02-5
1-phenylcyclopropanecarbonyl chloride

: 1191068-42-4
N-(4-aminobenzyl)-4-chloro-N-pyridin-2-ylmethylbenzenesulfonamide

: 1191067-77-2
1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1191068-31-1
4-chloro-N-(4-nitrobenzyl)-N-pyridin-2-ylmethylbenzenesulfonamide

: 1191067-77-2
1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride / iron / tetrahydrofuran; ethanol; water / 2 h / Reflux

2: triethylamine / dichloromethane / 0 - 20 °C

With ammonium chloride; triethylamine; iron; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 6120-95-2
1-phenyl-1-cyclopropane carboxylic acid

: 1191067-77-2
1-phenylcyclopropanecarboxylic acid (4-{[(4-chlorobenzenesulfonyl)-pyridin-2-ylmethylamino]methyl}phenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 3 h / Reflux

2: triethylamine / dichloromethane / 0 - 20 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;