(3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole
CAS No.:1224702-40-2
Molecular Formula:C₂₇H₃₅IN₂O₅
Molecular Weight:594.49
Hs Code.:

Synonyms:(3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

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Chemical Property of (3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

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Technology Process of (3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₃IN₂O₅

: 1224702-40-2
(3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 3h;
DOI:10.1002/ejoc.200901472

Reference yield: 66.0%

: 1224702-40-2
(3aR,5R,6S,6aR)-5-(benzylaminomethyl)-6-[(2-iodobenzyl)(tert-butoxycarbonyl)amino]-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

: 1224702-52-6
(2R,3R,3aS,11aR)-10-benzyl-4-(tert-butoxycarbonyl)-2,3-(isopropylidenedioxy)-3a,4,5,10,11,11a-hexahydrofuro[3,2-b][1,5]benzodiazocine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In toluene; for 19h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200901472