Technology Process of C22H18O5
There total 4 articles about C22H18O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; sodium hydrogencarbonate;
In
N,N-dimethyl-formamide;
at 100 - 200 ℃;
for 14h;
Inert atmosphere;
DOI:10.1080/00397911.2012.655358
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / water / Microwave irradiation
2: potassium carbonate / acetone / Reflux
3: palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 14 h / 100 - 200 °C / Inert atmosphere
With
dmap; palladium diacetate; sodium hydrogencarbonate; potassium carbonate;
In
water; N,N-dimethyl-formamide; acetone;
3: |Heck Reaction;
DOI:10.1080/00397911.2012.655358
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / water / Microwave irradiation
2: potassium carbonate / acetone / Reflux
3: palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 14 h / 100 - 200 °C / Inert atmosphere
With
dmap; palladium diacetate; sodium hydrogencarbonate; potassium carbonate;
In
water; N,N-dimethyl-formamide; acetone;
3: |Heck Reaction;
DOI:10.1080/00397911.2012.655358